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INEPT began life as an extension of early 2D 1H-13C correlation experiments1,2. These showed surprisingly good sensitivity, because of the twin advantages of polarization transfer from the higher ???protons and the shorter proton T1. It was then an obvious step to crystallise these advantages in a 1D experiment by removing the evolution period and adding refocusing pulses to make the technique broadband3. Two different experiments were performed, one generating antiphase peaks and the other refocused... Mehr